HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonal → HCID 86725131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonal | HCID 8438 | — |
| Reactant | HCID 71272057 | HCID 71272057 | — |
| Product | HCID 86725131 | HCID 86725131 | 72% |
Reaction Steps
(2Z)-3-(1,3-benzodioxol-5-yl)-2-{4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}prop-2-enenitrile is prepared starting from {4-[(11-hydroxyundecyl)oxy]-3-methoxyphenyl}acetonitrile and commercial 3,4-(methylenedioxy)benzaldehyde according the same procedure following for example 1 in 72% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-bab32462840546ee968938733db69739 |
| Source note | uspto-grants-2016_06 |