HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vanillin → 4-[(6-Hydroxyhexyl)oxy]-3-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vanillin | HCID 1183 | — |
| Reactant | 6-Chloro-1-hexanol | HCID 74828 | — |
| Product | 4-[(6-Hydroxyhexyl)oxy]-3-methoxybenzaldehyde | HCID 18008791 | 88% |
Reaction Steps
4-[(6-hydroxyhexyl)oxy]-3-methoxybenzaldehyde is prepared starting from 4-hydroxy-3-methoxybenzaldehyde and 6-chlorohexan-1-ol according the same procedure following for example 7 in 88% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-cd074e8007df40488ce0b8738a3ee121 |
| Source note | uspto-grants-2016_06 |