Ethylvanillin → HCID 86725133, compound

HRID 2204919Notes

Reaction equation

[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[OH:12])[CH:7]=[O:8])[CH3:2].Cl[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][OH:20]>>[CH2:1]([O:3][C:4]1[CH:5]=[C:6]([CH:9]=[CH:10][C:11]=1[O:12][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][OH:20])[CH:7]=[O:8])[CH3:2]

Participants

Reactant 2

HCID 8467Ethylvanillin

HCID 748286-Chloro-1-hexanol

Product 1

HCID 86725133HCID 86725133, compoundYield 84%

Procedure

3-ethoxy-4-[(6-hydroxyhexyl)oxy]benzaldehyde is prepared starting from 3-ethoxy-4-hydroxybenzaldehyde and 6-chlorohexan-1-ol according the same procedure following for example 7 in 84% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.

Sources & evidence

ORD record: ord-998e781c1b674f7bb482e243e1596eca
Source dataset: uspto-grants-2016_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09366906B2

Reaction notes

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