HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-(Methylenedioxy)phenylacetonitrile → HCID 71272496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-(Methylenedioxy)phenylacetonitrile | HCID 78178 | — |
| Reactant | HCID 86725133 | HCID 86725133 | — |
| Product | HCID 71272496 | HCID 71272496 | 96% |
Reaction Steps
(2Z)-2-(1,3-benzodioxol-5-yl)-3-{3-ethoxy-4-[(6-hydroxyhexyl)oxy]phenyl}prop-2-enenitrile is prepared starting from 3-ethoxy-4-[(6-hydroxyhexyl)oxy]benzaldehyde and 1,3-benzodioxol-5-ylacetonitrile according the same procedure following for example 10 in 96% yield. This material proves chromatographically homogenous and displays spectral characteristics consistent with its assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09366906B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-96aef3fe53dd43c38a5ac986cb82e110 |
| Source note | uspto-grants-2016_06 |