HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178441240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178441242 | HCID 178441242 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178441240 | HCID 178441240 | — |
Reaction Steps
To a solution of biphenyl imidazolyl tert-butyl ester (0,039 mmol, the title compound of Example 1445) in 0.5 mL of chloroform is added 0.25 mL of TFA, and the progress of the reaction is monitored by 1H NMR. The resulting solution is stirred at room temperature until the reaction is complete. The mixture is quenched with methanol and concentrated in vacuo. The residue is purified to give the title compound of Example 1446.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05426105 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-fd8718f9d29d4861b419fc48e473f608 |
| Source note | uspto-grants-1995_06 |