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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2205167Generated: November 1, 2026

4-Methoxybenzaldehyde → HCID 178497921, compound

https://huagongshe.com/reaction/2205167

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-MethoxybenzaldehydeHCID 31244—
ReactantBenzoic acid, 3-amino-, methyl esterHCID 78274—
SolventMethanolHCID 887—
ProductHCID 178497921HCID 17849792156.1%

Reaction Steps

4-Methoxybenzaldehyde (2.72 g, 19.98 mmol, 1.00 equiv), methyl 3-aminobenzoate (3 g, 19.85 mmol, 1.00 equiv), and methanol (30 mL) were placed in a 50-mL round-bottom flask and allowed to react, with stirring, at room temperature overnight. The resulting solids were collected by filtration and dried in an oven under reduced pressure, yielding 3 g (56%) of (E)-methyl 3-(4-methoxybenzylideneamino)benzoate as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09370522B2
Source datasetuspto-grants-2016_06
ORD IDord-e4bc40b409f1492182da3940fdb051e4
Source noteuspto-grants-2016_06