Potassium Hydroxide → HCID 53241517, compound

Participants

Reaction Steps

In a nitrogen atmosphere, methylcyclohexane (30 mL) and potassium hydroxide (3.1 g, 54.4 mmol) were added to a four-necked flask, and 3-(dimethylamino)-1,2-propanediol (0.72 g, 6.04 mmol: DAP) was dropped under agitation. Thereafter, linoleyl methane sulfonate (5.0 g, 14.5 mmol) was added, and agitation was performed at 40° C. for 13 hours. The reaction was terminated because remaining linoleyl methane sulfonate became 2.1% (degree of conversion: 68.0%, integrated value of isomer: 0.024).

Provenance & Evidence