Potassium Hydroxide → HCID 53241517, compound

Participants

Reaction Steps

In a nitrogen atmosphere, hexane (30 mL) and potassium hydroxide (6.1 g, 108.7 mmol) were put into a four-necked flask, and 3-(dimethylamino)-1,2-propanediol (0.72 g, 6.04 mmol: DAP) was dropped under agitation. Thereafter, linoleyl methane sulfonate (5.0 g, 14.5 mmol) was added, and agitation was performed at room temperature for 3 hours. The reaction was terminated because remaining linoleyl methane sulfonate became 0.2% (degree of conversion: 59.2%, integrated value of isomer: 0.027).

Provenance & Evidence