HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzofuran-2-sulfonyl chloride → HCID 68058401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzofuran-2-sulfonyl chloride | HCID 2795172 | — |
| Reactant | 2-((3-Nitrobenzyl)thio)aniline | HCID 4770810 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 68058401 | HCID 68058401 | 41.4% |
Reaction Steps
Following General Procedure B, the title compound (520 mg, 41%) was prepared from 2-((3-nitrobenzyl)thio)aniline (741 mg, 2.85 mmol), benzofuran-2-sulfonyl chloride (616 mg, 2.85 mmol) in pyridine (10 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371278B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-8832ff42eb434889a33f800f8a889a7b |
| Source note | uspto-grants-2016_06 |