HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tridecanoyl chloride → HCID 68286820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tridecanoyl chloride | HCID 87288 | — |
| Reactant | HCID 565168 | HCID 565168 | — |
| Reactant | (6S)-N-Benzyl-6-(4-hydroxybenzyl)-8-(naphthalen-1-ylmethyl)-4,7-dioxohexahydro-2H-pyrazino[1,2-a]pyrimidine-1(6H)-carboxamide | HCID 11295786 | — |
| Product | HCID 68286820 | HCID 68286820 | — |
Reaction Steps
According to particular aspects, synthesis of 44-(46S)-1-(benzylcarbamoyl)-8-(naphthalen-1-ylmethyl)-4,7-dioxooctahydro-1H-pyrazino[1,2-a]pyrimidin-6-yl)methyl)phenyl palmitate was achieved in analogy with above Example 10 except starting with a solution of (6 S)—N-benzyl-6-(4-hydroxybenzyl)-8-(naphthalen-1-ylmethyl)-4,7-dioxooctahydro-1H-pyrazino[1,2-a]pyrimidine-1-carboxamide, and reacting with tridecanoyl chloride to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371330B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-b7efe7fc91b0428eb497c87a3d6a0a17 |
| Source note | uspto-grants-2016_06 |