HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178441908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 178441910 | HCID 178441910 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178441908 | HCID 178441908 | — |
Reaction Steps
To a solution of biphenyl indolizinyl tert-butyl ester (0.039 mmol, the title compound of Example 3231) in 0.5 mL of chloroform is added 0.25 mL of TFA, and the progress of the reaction is monitored by 1H NMR. The resulting solution is stirred at room temperature until the reaction is complete. The mixture is quenched with methanol and concentrated in vacuo. The residue is purified to give the title compound of Example 3232.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05426105 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-6cbf27641065418bbebb0d5af5ea365e |
| Source note | uspto-grants-1995_06 |