Thionyl Chloride → HCID 68595408, compound

Participants

Reaction Steps

Add thionyl chloride (0.4 mL, 5.49 mmol) to a solution of {4-[4-(3-Methyl-1-phenyl-1H-pyrazol-4-ylmethyl)-3,4,5,6-tetrahydro-2H-[1,2′]bipyrazinyl-3′-yl]-phenyl}-methanol (474 mg, 1.08 mmol) in DCM (20 mL). Maintain stirring for 3 hr. Concentrate to dryness to give the title compound as a yellow material (545 mg) MS (ES): m/z=459/460/461[M+H]+.

Provenance & Evidence