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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2205737Generated: November 1, 2026

Hydrazine hydrate (1:1) → HCID 58118989, compound

https://huagongshe.com/reaction/2205737

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
ReactantHCID 55127404HCID 55127404—
ProductHCID 58118989HCID 58118989—

Reaction Conditions

Temperature120 °C

Reaction Steps

A sealable flask is charged with 2-(benzyloxymethyl)-3,6-dichloropyridine as prepared in Step 2 (950 mg, 3.5 mmol), hydrazine hydrate (1 mL) is added, and the reaction is heated to 120° C. overnight. After cooling the solids are collected by filtration to provide 2-(benzyloxymethyl)-3-chloro-6-hydrazinylpyridine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09371329B2
Source datasetuspto-grants-2016_06
ORD IDord-d9fef2af494e46a688c9f94eaf38a426
Source noteuspto-grants-2016_06