3,4-Dimethoxyaniline → HCID 86706293, compound

Participants

Reaction Steps

The title compound was prepared in 71% yield from compound (10) and 3,4-dimethoxyphenyl amine using the method described for Preparation 35. 1H-NMR (CDCl3, 500 MHz): δ 1.46 (s, 9H), 1.68 (s, 9H), 3.90 (s, 3H), 3.91 (s, 3H), 6.45 (br s, 1H, NH), 6.56 (d, J=0.95 Hz, 1H), 6.89 (m, 2H), 6.96 (m, 1H), 7.45 (m, 1H), 7.81 (d, J=0.63 Hz, 1H), 8.20 (d, J=0.95 Hz, 1H), 8.42 (d, J=0.95 Hz, 1H).

Provenance & Evidence