2-Chloro-4-methoxyaniline → HCID 86706294, compound

Participants

Reaction Steps

The title compound was prepared in 72% yield from compound (10) and 2-chloro-4-methoxyphenylamine using the method described for Preparation 35. 1H-NMR (CDCl3, 500 MHz): δ 1.49 (s, 9H), 1.69 (s, 9H), 3.82 (s, 3H), 6.58 (d, J=0.95 Hz, 1H over br s, 1H), 6.86 (dd, J=2.84, 8.83 Hz, 1H), 7.03 (d, J=2.84 Hz, 1H), 7.38 (m, 1H), 7.73 (d, J=9.14 Hz, 1H), 7.82 (d, J=0.63 Hz, 1H), 8.21 (d, J=0.63 Hz, 1H), 8.46 (d, J=0.63 Hz, 1H).

Provenance & Evidence