o-Phenetidine → HCID 86706296, compound

Participants

Reaction Steps

The title compound was prepared in 33% yield from compound (10) and 2-ethoxyphenylamine using the method described for Preparation 35. 1H-NMR (CDCl3, 500 MHz): δ 1.48 (t, J=6.94 Hz, 3H), 1.54 (s, 9H), 1.69 (s, 9H), 4.14 (q, J=6.94 Hz, 2H), 6.59 (d, J=0.63 Hz, 1H), 6.91-6.98 (m, 3H), 7.11 (br s, 1H), 7.70 (m, 1H), 7.83 (d, J=0.63 Hz, 1H), 7.91 (br d, J=8.20 Hz, 1H), 8.33 (d, J=0.63 Hz, 1H), 8.49 (s, 1H).

Provenance & Evidence