4-(2-Methoxyethoxy)aniline → HCID 86706301, compound

Participants

Reaction Steps

The title compound was prepared in 27% yield from compound (17) and 4-(2-methoxyethoxy)aniline using the method described for compound (49). 1H-NMR (500 MHz, DMSO-d6) 1.45 (s, 9H), 1.60 (s, 9H), 3.31 (s, 3H), 3.64 (t, J=5.0 Hz, 2H), 4.04 (t, J=5.0 Hz, 2H), 6.79 (s, 1H), 6.88 (d, J=9.0 Hz, 2H), 7.40 (s, 1H), 7.48 (d, J=9.0 Hz, 2H), 8.01 (d, J=0.5 Hz, 1H), 8.41 (d, J=0.9 Hz, 1H), 8.44 (s, 1H), 8.74 (s, 1H).

Provenance & Evidence