HCID 67255784, compound → HCID 67254470, compound

Participants

Reaction Steps

10% Pd on carbon (12 mg, 0.866 mmol) was added to a solution of tert-butyl 3-methoxy-4-nitrobenzyl(methyl)carbamate (Preparation 107, 185 mg, 0.62 mmol) in EtOH (3 mL). The reaction mixture was degassed and then stirred for 1 hour at room temperature under an atmosphere of hydrogen. The reaction was filtered on a pad of Celite and the filtrate was concentrated under reduced pressure to afford the title compound (0.16 g, 96%).

Provenance & Evidence