Triacetoxyperiodinane → HCID 117987725, compound

Participants

Reaction Steps

To a solution of (5-bromo-3-fluoro-2-methoxypyridin-4-yl)(cyclopentyl)methanol (430 mg) in acetonitrile (10 mL) was added Dess-Martin reagent (720 mg) at room temperature, and the mixture was stirred for 3 hr, and the reaction mixture was concentrated under reduced pressure. The residue was purified by silica gel column chromatography (basic silica gel, ethyl acetate/hexane) to give the title compound (440 mg).

Provenance & Evidence