反应详情

Of the compound from Example 12A, 248 mg (1.04 mmol) were introduced in methanol and admixed with 20 mg of palladium (10% on activated carbon). Hydrogenation took place under atmospheric pressure at RT overnight. The reaction mixture was filtered and the filtrate concentrated under reduced pressure. This gave 300 mg (88% of theory) of the title compound.

1. customat RT
2. customovernight
3. filtrationThe reaction mixture was filtered
4. concentrationthe filtrate concentrated under reduced pressure