HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10426278, compound → HCID 68810359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10426278 | HCID 10426278 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 68810359 | HCID 68810359 | — |
Reaction Steps
((1S)-1-benzyl-3-ethylamino-2-hydroxy-3-oxopropyl)carbamic acid 1,1-dimethylethyl ester (5.5 g, 17 mmol) was dissolved in 4N hydrochloric acid/dioxane solution (65 mL), and the solution was stirred at room temperature for 3 hours. This solution was concentrated in vacuo to quantitatively yield the title compound (4.4 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371359B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-296c9784e72f41f7a4d2684758cb2330 |
| Source note | uspto-grants-2016_06 |