Hydrochloric Acid → HCID 118511016, compound

Participants

Reaction Conditions

Reaction Steps

The synthesized 2-naphthoyl methoxy pyrene (30.9 g, 0.08 mol), 1-dodecanethiol (48.58 g, 0.24 mol), potassium hydroxide (16.8 g, 0.3 mol), and N,N-dimethylformamide (350 g) were put in a flask and then agitated at 100° C. for 2 hours. The reaction mixture was cooled down to ambient temperature and agitated and then neutralized to about pH 7 by adding a 10% hydrogen chloride (hydrochloric acid) solution thereto. Then, the resultant was extracted by using ethyl acetate, obtaining 2-naphthoyl hydroxy pyrene.

Provenance & Evidence