HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 53380482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 71110697 | HCID 71110697 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53380482 | HCID 53380482 | 55.2% |
Reaction Steps
To a suspension of 151 (380 mg, 0.68 mmol) in CH3OH (5.0 mL) was added K2CO3 (65 mg, 0.47 mmol) at room temperature. After 1.5 h, the resulting mixture was filtered, and then purified by preparative HPLC (reverse phase) to provide the title compound (145 mg, 55%) as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371303B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-8d7e32e0cc944b19877f0964e257e2f6 |
| Source note | uspto-grants-2016_06 |