HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2206821Generated: October 28, 2026
HCID 169993, compound → HCID 86702299, compound
https://huagongshe.com/reaction/2206821
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 169993 | HCID 169993 | — |
| Reactant | HCID 178418486 | HCID 178418486 | — |
| Product | HCID 86702299 | HCID 86702299 | — |
Reaction Steps
A round bottom flask was charged with chlorodecyldimethylsilane (12.362 g; 50.00 mmol) and the flask was cooled with an ice-water bath to 0° C. Ethynylmagnesium bromide (0.5M in THF, 125.0 cm3, 62.50 mmol) was added into the flask over 30 min. The cooling bath was removed and the mixture was stirred at 50° C. for an additional hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09373801B2 |
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| Source dataset | uspto-grants-2016_06 |
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| ORD ID | ord-4b9c02dc51a14636898a9b18a9319902 |
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| Source note | uspto-grants-2016_06 |
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