HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzeneacetamide → HCID 71459139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzeneacetamide | HCID 7680 | — |
| Reactant | Benzenepropanal | HCID 7707 | — |
| Reactant | HCID 71457306 | HCID 71457306 | — |
| Product | HCID 71459139 | HCID 71459139 | 92% |
Reaction Steps
Compound 45 was prepared from 2-phenylacetamide and 3-phenylpropanal using the procedure for compound 44. Yield: 92%. 1HNMR (400 MHz, DMSO-d6) δ 8.45 (d, J=7.6 Hz, 2H), 7.10-7.31 (m, 15H), 5.26 (t, J=7.6 Hz, 1H), 3.38-3.46 (m, 4H), 2.47-2.53 (m, 2H), 1.88-1.94 (m, 2H). LC-MS (ESI): m/z 387.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376380B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-9964ae91178148a6a4ffe02e66c5d802 |
| Source note | uspto-grants-2016_06 |