HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylacetamide → HCID 71455515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylacetamide | HCID 12957 | — |
| Reactant | 4-(Diethylamino)benzaldehyde | HCID 67114 | — |
| Product | HCID 71455515 | HCID 71455515 | 77% |
Reaction Steps
Compound 51 was prepared from pivalamide and 4-(diethylamino)benzaldehyde using method 1. Yield: 77%. 1H NMR (400 MHz, DMSO) δ 7.70 (d, J=8.8 Hz, 2H), 7.03 (d, J=8.8 Hz, 2H), 6.62 (d, J=8.8 Hz, 2H), 6.52 (t, J=8.4 Hz, 1H), 3.30-3.33 (m, 4H), 1.12 (s, 18H), 1.05-1.08 (m, 6H). LC-MS (ESI): m/z 262.2 (M+H)+. HRMS (ESI) for C21H36N3O2 (MH+): calcd, 362.2802. found 362.2795.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376380B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-1060ddd0dcf84de0aa8f70219181f38f |
| Source note | uspto-grants-2016_06 |