4-(Diethylamino)benzaldehyde → N,N'-((4-(diethylamino)phenyl)methylene)dioctanamide

Participants

Reaction Steps

Compound 54 was prepared from octanamide and 4-(diethylamino)benzaldehyde using method 1. Yield: 68%. 1H NMR (400 MHz, DMSO) δ 8.21 (d, J=8.0 Hz, 2H), 7.07 (d, J=8.8 Hz, 2H), 6.61 (d, J=8.8 Hz, 2H), 6.42 (t, J=8.0 Hz, 1H), 3.29-3.31 (m, 4H), 2.06-2.14 (m, 4H), 1.47-1.50 (m, 4H), 1.08-1.24 (m, 16H), 1.06 (t, J=7.2 Hz, 6H), 0.94 (t, J=7.2 Hz, 6H). LC-MS (ESI): m/z 446.3 (M+H)+. HRMS (ESI) for C27H48N3O2 (MH+): calcd, 446.3741. found 446.3734.

Provenance & Evidence