HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzylamine → 4-(o-Tolylmethylamino)but-3-en-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzylamine | HCID 6993 | — |
| Reactant | 3-Buten-2-one, 4-methoxy- | HCID 94297 | — |
| Product | 4-(o-Tolylmethylamino)but-3-en-2-one | HCID 90303972 | — |
Reaction Steps
The title compound 60 is prepared according to the procedure reported in step A of Example 18 with 4-methoxy-3-buten-2-one (0.1 g, 1 mmol) and 2-methylbenzylamine (0.125 g, 1 mmol) as reactants. Yellow solid. (Yield 0.19 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-1bc6bd502f5343af9cb28706471cb2bf |
| Source note | uspto-grants-2016_06 |