HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90304014, compound → HCID 118557931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90304014 | HCID 90304014 | — |
| Reactant | HCID 131735879 | HCID 131735879 | — |
| Product | HCID 118557931 | HCID 118557931 | — |
Reaction Steps
The title compound 73 is prepared according to the procedure reported in step D of Example 8 with aldehyde 76 (121 mg, 0.47 mmol) and enamine 45 (138 mg, 0.56 mmol) as reactants. Purification by column chromatography on SiO2 (Petroleum Ether/EtOAc=2:1) afford the title compound 74 as a yellow oil. (Yield 67.5 mg, 32%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-e2969e26d1b94f96855e1c6ad7445117 |
| Source note | uspto-grants-2016_06 |