反应详情

Hydrogen was passed through a degassed solution of 4-azidomethyl-3-fluorobenzoic acid methyl ester from Example E3.3 (2.11 g, 10 mmol) in methanol containing 10% palladium on carbon for 2 h. The reaction mixture was filtered through Celite® filter agent and the filtrate was concentrated in vacuo to give a colourless oil identified as the title compound (1.51 g, 83%).

1. filtrationThe reaction mixture was filtered through Celite®
2. filtrationfilter agent
3. concentrationthe filtrate was concentrated in vacuo
4. customto give a colourless oil