HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 118071535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 118074739 | HCID 118074739 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 118071535 | HCID 118071535 | — |
Reaction Steps
To a mixture of tert-butyl (6-bromo-2,3-dihydro-1-benzofuran-5-yl)carbamate (2.75 g) and dioxane (15.0 mL) was added hydrogen chloride (4 M dioxane solution, 15.0 mL), followed by stirring at room temperature overnight. The solvent was evaporated under reduced pressure to obtain 6-bromo-2,3-dihydro-1-benzofuran-5-amine hydrochloride (2.23 g) as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376449B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-a8a0f8b9f738454aae043c352651820b |
| Source note | uspto-grants-2016_06 |