m-Chlorophenylhydrazine hydrochloride → HCID 118431884, compound

HRID 2207963Notes

Reaction equation

HRID 2207963 reaction equation
[F:1][C:2]([F:25])([C:21]([F:24])([F:23])[F:22])[C:3](=O)[CH:4]=[CH:5][C:6]1[CH:7]=[C:8]([C:12]2[CH:17]=[CH:16][C:15]([S:18][CH3:19])=[CH:14][CH:13]=2)[CH:9]=[CH:10][CH:11]=1.Cl.[Cl:27][C:28]1[CH:29]=[C:30]([NH:34][NH2:35])[CH:31]=[CH:32][CH:33]=1>>[Cl:27][C:28]1[CH:29]=[C:30]([N:34]2[CH:5]([C:6]3[CH:7]=[C:8]([C:12]4[CH:17]=[CH:16][C:15]([S:18][CH3:19])=[CH:14][CH:13]=4)[CH:9]=[CH:10][CH:11]=3)[CH2:4][C:3]([C:2]([F:25])([F:1])[C:21]([F:24])([F:23])[F:22])=[N:35]2)[CH:31]=[CH:32][CH:33]=1

Participants

3

Reactant 2

HCID 75331m-Chlorophenylhydrazine hydrochlorideHCID 131735937HCID 131735937, compound

Product 1

HCID 118431884HCID 118431884, compound

Procedure

The titled compound was prepared in accordance with the same procedures as in Example 23, except for using 4,4,5,5,5-pentafluoro-1-(4′-methylsulfanyl-biphenyl-3-yl)-pent-1-en-3-one prepared in Step 3 of Preparation 4; and using 3-chlorophenylhydrazine hydrochloride instead of 4-chlorophenylhydrazine hydrochloride.

Sources & evidence

ORD record
ord-17d14d38f02d44d5870d7650d0d6dbd4
Source dataset
uspto-grants-2016_06
Patent number
US09376420B2

Reaction notes

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