HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanogen Bromide → HCID 178508298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanogen Bromide | HCID 10476 | — |
| Reactant | HCID 86725249 | HCID 86725249 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178508298 | HCID 178508298 | — |
Reaction Steps
To (R)-3-(2-(3,4-bis(aminomethyl)benzamido)-2-boronoethyl)-2-hydroxybenzoic acid (10 mg) in DMF (1 mL) was added BrCN (10 mg) and the reaction was stirred for 5 hr. The crude product was purified by reverse phase preparative HPLC and dried using lyophilization. ESI-MS m/z 395 (MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376454B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-aef5ae5541204238ab16c99b4f7b0298 |
| Source note | uspto-grants-2016_06 |