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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 22088Generated: October 25, 2026

4-Coumaric acid → 2-Propenoic acid, 3-phenyl-

https://huagongshe.com/reaction/22088

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Coumaric acidHCID 322—
ReactantGlycerolHCID 753—
ReactantBoron trifluoride etherateHCID 8000—
ReactantGlycidolHCID 11164—
SolventDimethyl SulfoxideHCID 679—
Product2-Propenoic acid, 3-phenyl-HCID 8784—

Reaction Conditions

Temperature90 °C

Reaction Steps

8.719 g of p-hydroxy cinnamic acid was dissolved in 10 ml of DMSO, and 19.7 g of glycidol was added. The mixture was stirred and heated to 90° C. Catalystic amount of boron trifluoride ethyl ether was added, heating and agitation was carried out for 2 hours and then the adduct of cinnamic acid and glycerin was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05426210
Source datasetuspto-grants-1995_06
ORD IDord-12a47bbc2fa647d09b787ad23f92c3fb
Source noteuspto-grants-1995_06