m-Chloroperbenzoic acid → HCID 70874731, compound

Participants

Reaction Conditions

Reaction Steps

To a stirred solution of 5-chloro-3-(cyclohexylthio)-N-((4,6-dimethyl-2-oxo-1,2-dihydropyridin-3-yl)methyl)-2-methylbenzamide (0.2 g, 0.48 mmol) in DCM (7 mL) at 0° C., m-CPBA (0.098 g, 0.57 mmol) was added and stirred at 0° C. for 2 h. Reaction was monitored by TLC. After completion, the reaction mixture was diluted with DCM and washed with aqs. NaHCO3. The product was purified by solvent washings to afford the title compound (0.17 g, 82.3%).

Provenance & Evidence