HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Propenoic acid, 3-phenyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Coumaric acid | HCID 322 | — |
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Glycerol | HCID 753 | — |
| Product | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
Reaction Steps
8.719 g of p-hydroxy cinnamic acid was dissolved in 10 ml of DMSO, and 100 mg of sodium hydroxide was added. The mixture was stirred and heated to 90° C. under a flow of N2 gas. 19.7 g of glycidol was added gradually, heating and agitation was carried out for 2 hours, neutralized by adding hydrochloric acid and then the adduct of cinnamic acid and glycerin was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05426210 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-b76ea8f01bb84b6080b39c1bfb6ab1c0 |
| Source note | uspto-grants-1995_06 |