Benzylamine → HCID 178482889, compound

HRID 2209778Notes

Reaction equation

HRID 2209778 reaction equation
[C:1]([O:5][C:6]([C:8]1[CH:13]=[CH:12][C:11]([CH:14]2[CH2:19][CH2:18][C:17](=O)[CH2:16][CH2:15]2)=[C:10]([CH2:21][NH:22][CH3:23])[CH:9]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:24]([NH2:31])[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[CH2:24]([NH:31][C@H:17]1[CH2:18][CH2:19][C@H:14]([C:11]2[CH:12]=[CH:13][C:8]([C:6]([O:5][C:1]([CH3:4])([CH3:3])[CH3:2])=[O:7])=[CH:9][C:10]=2[CH2:21][NH:22][CH3:23])[CH2:15][CH2:16]1)[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 67847118HCID 67847118, compound

Product 1

HCID 178482889HCID 178482889, compound

Procedure

from 4-(4-tert.butoxycarbonyl-methylaminomethylphenyl)-cyclohexanone and benzylamine. Colourless oil. Rf value: 0.45 (alumina, petroleum ether/ethyl acetate=2:1, v:v).

Sources & evidence

ORD record
ord-6face49763e54b1a9fc9e6b728187f02
Source dataset
uspto-grants-1995_10
Patent number
US05455273

Reaction notes

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