HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178482896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | HCID 178482895 | HCID 178482895 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178482896 | HCID 178482896 | 91.1% |
Reaction Steps
8 g (0.024 Mol) of trans-4-(4-tert.butoxycarbonyl-methylaminomethylphenyl)-N-methylcyclohexylamine are reacted in 300 ml of ether with 4.6 g (0.026 Mol) of 4-chlorobenzoylchloride in the presence of 2.7 g (0.026 Mol) of triethylamine. 10.3 g of the title compound are obtained, melting point 152°-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05455273 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-57393db1a82a46e9b1fc949479e5a2e8 |
| Source note | uspto-grants-1995_10 |