4-Chlorobenzoyl chloride → HCID 178483967, compound

HRID 2209783Notes

Reaction equation

HRID 2209783 reaction equation
[C:1]([O:5][C:6]([CH:8]([C:12]1[CH:17]=[CH:16][C:15]([C@H:18]2[CH2:23][CH2:22][C@H:21]([NH:24][CH3:25])[CH2:20][CH2:19]2)=[CH:14][CH:13]=1)[CH2:9][NH:10][CH3:11])=[O:7])([CH3:4])([CH3:3])[CH3:2].[Cl:26][C:27]1[CH:35]=[CH:34][C:30]([C:31](Cl)=[O:32])=[CH:29][CH:28]=1>>[C:1]([O:5][C:6]([CH:8]([C:12]1[CH:17]=[CH:16][C:15]([C@H:18]2[CH2:23][CH2:22][C@H:21]([N:24]([C:31](=[O:32])[C:30]3[CH:34]=[CH:35][C:27]([Cl:26])=[CH:28][CH:29]=3)[CH3:25])[CH2:20][CH2:19]2)=[CH:14][CH:13]=1)[CH2:9][NH:10][CH3:11])=[O:7])([CH3:3])([CH3:4])[CH3:2]

Participants

3

Reactant 2

HCID 85014-Chlorobenzoyl chlorideHCID 178483966HCID 178483966, compound

Product 1

HCID 178483967HCID 178483967, compound

Procedure

from trans-4-[4-(1-tert.butoxycarbonyl-methylaminoethyl)-phenyl]-N-methylcyclohexylamine and 4-chlorobenzoylchloride. Melting point: 172°-174° C.

Sources & evidence

ORD record
ord-c7706ec07a7743b79e6898f51ee9af5a
Source dataset
uspto-grants-1995_10
Patent number
US05455273

Reaction notes

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