4-Chlorobenzoyl chloride → HCID 178482969, compound

HRID 2209784Notes

Reaction equation

HRID 2209784 reaction equation
[C:1]([O:5][C:6]([C:8]1[C:9]([CH2:22][NH:23][CH3:24])=[C:10]([C@H:14]2[CH2:19][CH2:18][C@H:17]([NH:20][CH3:21])[CH2:16][CH2:15]2)[CH:11]=[CH:12][CH:13]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[Cl:25][C:26]1[CH:34]=[CH:33][C:29]([C:30](Cl)=[O:31])=[CH:28][CH:27]=1>>[C:1]([O:5][C:6]([C:8]1[C:9]([CH2:22][NH:23][CH3:24])=[C:10]([C@H:14]2[CH2:15][CH2:16][C@H:17]([N:20]([C:30](=[O:31])[C:29]3[CH:33]=[CH:34][C:26]([Cl:25])=[CH:27][CH:28]=3)[CH3:21])[CH2:18][CH2:19]2)[CH:11]=[CH:12][CH:13]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 85014-Chlorobenzoyl chlorideHCID 178482968HCID 178482968, compound

Product 1

HCID 178482969HCID 178482969, compound

Procedure

from trans-4-(3-tert.butoxycarbonyl-methylaminomethylphenyl)-N-methylcyclohexylamine and 4-chlorobenzoylchloride. Melting point: 134°-135° C.

Sources & evidence

ORD record
ord-1ab71c3b8ae74148b1f2617bcde57790
Source dataset
uspto-grants-1995_10
Patent number
US05455273

Reaction notes

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