HCID 53909576, compound → HCID 178465095, compound

HRID 2209797Notes

Reaction equation

HRID 2209797 reaction equation
[C:1]([O:5][C:6]([C:8]1[CH:13]=[CH:12][C:11]([C@H:14]2[CH2:19][CH2:18][C@H:17]([NH:20][CH2:21][CH3:22])[CH2:16][CH2:15]2)=[C:10]([CH2:23][NH:24][CH3:25])[CH:9]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[C:26]1([CH:32]=[CH:33][CH2:34][C:35](Cl)=[O:36])[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[C:1]([O:5][C:6]([C:8]1[CH:13]=[CH:12][C:11]([C@H:14]2[CH2:15][CH2:16][C@H:17]([N:20]([CH2:21][CH3:22])[C:35](=[O:36])[CH2:34][CH:33]=[CH:32][C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)[CH2:18][CH2:19]2)=[C:10]([CH2:23][NH:24][CH3:25])[CH:9]=1)=[O:7])([CH3:2])([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 53909576HCID 53909576, compoundHCID 178464516HCID 178464516, compound

Product 1

HCID 178465095HCID 178465095, compound

Procedure

from trans-4-(4-tert.butoxycarbonyl-methylaminomethylphenyl)-N-ethylcyclohexylamine and 4-phenyl-3-butenoylchloride. Colourless oil. Rf value: 0.74 (alumina, petroleum ether/ethyl acetate=2:1, v:v).

Sources & evidence

ORD record
ord-fa508b95b520415785a7ea2235c32be6
Source dataset
uspto-grants-1995_10
Patent number
US05455273

Reaction notes

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