Ethanol, 1-bromo- → HCID 178464196, compound

HRID 2209812Notes

Reaction equation

HRID 2209812 reaction equation
[Cl:1][C:2]1[CH:27]=[CH:26][C:5]([C:6]([N:8]([C@H:10]2[CH2:15][CH2:14][C@H:13]([C:16]3[CH:21]=[CH:20][C:19]([CH:22]([NH:24][CH3:25])[CH3:23])=[CH:18][CH:17]=3)[CH2:12][CH2:11]2)[CH3:9])=[O:7])=[CH:4][CH:3]=1.Br[CH:29]([OH:31])[CH3:30]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([C:6]([N:8]([C@H:10]2[CH2:11][CH2:12][C@H:13]([C:16]3[CH:17]=[CH:18][C:19]([CH:22]([NH:24][CH2:25][CH2:30][CH2:29][OH:31])[CH3:23])=[CH:20][CH:21]=3)[CH2:14][CH2:15]2)[CH3:9])=[O:7])=[CH:26][CH:27]=1

Participants

3

Reactant 2

HCID 14202443Ethanol, 1-bromo-HCID 178483201HCID 178483201, compound

Product 1

HCID 178464196HCID 178464196, compound

Procedure

from trans-N-(4-chlorobenzoyl)-N-methyl-4-[4-(1-methylaminoethyl)phenyl]cyclohexylamine and bromoethanol. Melting point: 118°-120° C.

Sources & evidence

ORD record
ord-401d2ccc511e4e3992734259b72944bb
Source dataset
uspto-grants-1995_10
Patent number
US05455273

Reaction notes

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