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Trichloro(chloromethyl)silane → Chloromethyldichloro(4-fluorophenyl)silane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trichloro(chloromethyl)silane | HCID 15258 | — |
| 反応物 | HCID 178418676 | HCID 178418676 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | Chloromethyldichloro(4-fluorophenyl)silane | HCID 19382008 | — |
反応手順
In the same apparatus as Example 1, was added 5.6 g of chloromethyltrichlorosilane (0.03 mol) and 50 ml of THF. Through the dropping funnel was firstly added 22 ml of 4-fluorophenylmagnesiumbromide (2.0 M in diethylether) to give chloromethyldichloro(4-fluorophenyl)silane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05455356 |
| 出典データセット | uspto-grants-1995_10 |
| ORD ID | ord-9a42c4cfd268423fa50241803e4fe507 |
| 出典メモ | uspto-grants-1995_10 |