HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 12493615, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 21613252 | HCID 21613252 | — |
| Product | HCID 12493615 | HCID 12493615 | — |
Reaction Steps
Pyrrolidine (28.5 g) is cooled on an ice bath. 1,3,5-Trichlorotriazine (18.4 g) is added with vigorous stirring. After 1-1.5 h the mixture is permitted to warm to 20°-25°. The solid is filtered and rinsed several times with water and dried under reduced pressure to give the monochloro-bis(1-pyrrolidinyl)triazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE035053 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-9c9417b9d1b24eea86d31cbe87b4f598 |
| Source note | uspto-grants-1995_10 |