HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromohexane → HCID 10765979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromohexane | HCID 8101 | — |
| Reactant | Potassium Bicarbonate | HCID 516893 | — |
| Reactant | HCID 10021812 | HCID 10021812 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 10765979 | HCID 10765979 | — |
Reaction Steps
0,183 g (0.5 mmol) of the compound of Example 1 and 0.25 g (2.5 mmol) of potassium hydrogen carbonate are stirred for a few moments in 10 ml of dimethylformamide at 110° C. under nitrogen until they have completely dissolved. 0.7 ml(5 mmol) of [1-bromo-n-hexane] are then added and the reaction is continued under the same conditions for two hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05457103 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-1142335aba98410a967357d45504c7c6 |
| Source note | uspto-grants-1995_10 |