HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 13170235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 8-Methoxy-2-tetralone | HCID 4136021 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13170235 | HCID 13170235 | — |
Reaction Steps
To 75 mL of toluene were added 3.52 gm (20 mMol) of 8-methoxy-2-tetralone followed by 2.5 gm of pyrrolidine. The mixture was heated to reflux for 3 hours after which the solvent was evaporated in vacuo to give 3-pyrrolidino-5-methoxy-1,2-dihydronaphthalene as a dark oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05457121 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-cc40d7a422f243f3a79a23baf5323858 |
| Source note | uspto-grants-1995_10 |