HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5-methylpyridine-2-sulfonamide → HCID 19378715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5-methylpyridine-2-sulfonamide | HCID 19378709 | — |
| Reactant | Ethylorthoformate | HCID 53630039 | — |
| Product | HCID 19378715 | HCID 19378715 | — |
Reaction Steps
A suspension of 1.3 g of 3-amino-5-methylpyridine-2-sulfonamide (Preparation 25) in 13 cm3 of ethyl orthoformate is brought to reflux for 2 hours. After cooling, the precipitate obtained is collected on a filter, washed with diethyl ether and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459138 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-7f7baae9d7d847aaa5f1af257c414a17 |
| Source note | uspto-grants-1995_10 |