HCID 19379092, compound → HCID 19379065, compound

Participants

Reaction Steps

Following the procedure of Nacci et al, Vide Supra, reaction of 4-(3-cyclopentylmethyl-4-methoxyphenyl)-2,6-piperidinedione (20.0 mmol, 6.0 g) and lithium aluminum hydride (209 mmol, 7.94 g) in dry THF (130 mL) afforded the title compound as a white, waxy solid (4.85 g, 89%) of sufficient purity for subsequent transformations.

Provenance & Evidence