HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 44211848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 67624507 | HCID 67624507 | — |
| Product | HCID 44211848 | HCID 44211848 | 69.5% |
Reaction Steps
684 mg of 2-ethyl-3-(2'-methoxalylbiphenyl-4-yl)methyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridine [prepared as described in step (a) above] were subjected to hydrolysis using 201 mg of lithium hydroxide monohydrate in the same manner as described in Example 1(b), to give 460 mg of the title compound as a powder, melting at 209°-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459148 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-0cb728b1c8594a3facb04c5226adb4d1 |
| Source note | uspto-grants-1995_10 |