HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 14518105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | Aminoacetaldehyde dimethyl acetal | HCID 89728 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14518105 | HCID 14518105 | 99.7% |
Reaction Steps
A mixture of 4.2 g of 2,2-dimethoxyethanamine, 3.6 g of isothiocyanatomethane and 100 ml of tetrahydrofuran was stirred overnight. The reaction mixture was evaporated, yielding 7.1 g (99%) of N-(2,2-dimethoxyethyl)-N'-methylthiourea as an oily residue (interm. 34);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05461050 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-9bfb0dcacdfc4b46bd67dd709ee3b9d7 |
| Source note | uspto-grants-1995_10 |